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精萘厂家:提取的方法

来源:http://www.jnjdbc.cn/ 日期:2024-11-23 发布人:创始人

  精萘的提取可以通过多种方法进行,以下是几种常见的精萘提取方法:

  The extraction of refined naphthalene can be carried out through various methods, and the following are several common methods for extracting refined naphthalene:

  煤焦油提取法 :

  Coal tar extraction method:

  从高温煤焦油中分离出萘油馏分(210-230℃),经过洗涤脱酚和精馏分离轻组分,得到工业萘。

  Separate naphthalene oil fraction (210-230 ℃) from high-temperature coal tar, wash and dephenolate, and separate light components by distillation to obtain industrial naphthalene.

  工业萘进一步通过酸洗和蒸馏,硫含量可降至小于0.1%,再通过加氢精制工艺,硫含量可低于0.05%。

  Industrial naphthalene can further reduce its sulfur content to less than 0.1% through acid washing and distillation, and then through hydrogenation refining process, its sulfur content can be reduced to less than 0.05%.

  结晶法 :

  Crystallization method:

  利用不同纯度萘的熔点差异,通过分步结晶和融化操作,高结晶点萘进入成品槽,低纯度萘进入残油罐。

  By utilizing the melting point differences of different purity naphthalenes, high crystallization point naphthalenes enter the finished product tank and low purity naphthalenes enter the residual oil tank through step-by-step crystallization and melting operations.

  在精制工序中,通过闪蒸进一步精制制得精萘。

  In the refining process, refined naphthalene is further refined by flash evaporation.

  溶剂萃取法 :

  Solvent extraction method:

  使用乙醇对煤焦油进行萃取,然后对萃出液减压蒸馏,得到含萘量较高的固液混合物,经过滤抽干得到粗萘。

  Ethanol is used to extract coal tar, and then the extracted liquid is subjected to vacuum distillation to obtain a solid-liquid mixture with high naphthalene content. After filtration and dehydration, crude naphthalene is obtained.

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  水蒸汽蒸馏法 :

  Steam distillation method:

  建立水蒸汽蒸馏提纯粗萘的方法,所得精萘纯度可达99.48%,回收率在93%以上。

  Establishing a method for steam distillation purification of crude naphthalene, the purity of refined naphthalene obtained can reach 99.48%, with a recovery rate of over 93%.

  分步结晶法 :

  Stepwise crystallization method:

  将工业萘装入箱式结晶器中,根据萘中各馏分结晶点的差别进行分步结晶提纯。

  Load industrial naphthalene into a box type crystallizer and perform step-by-step crystallization purification based on the differences in crystallization points of each fraction in naphthalene.

  竖管式结晶法 :

  Vertical tube crystallization method:

  利用竖管式结晶器进行多级结晶过程,包括结晶、发汗和熔融步骤,生产出高纯度的精萘。

  Using a vertical tube crystallizer for multi-stage crystallization process, including crystallization, sweating, and melting steps, high-purity refined naphthalene is produced.

  反应与精馏结合法 :

  Reaction and distillation combined method:

  以工业萘为原料,通过过氧化氢氧化和有机酸、无机酸催化,结合精馏方法提取精萘。

  Using industrial naphthalene as raw material, refined naphthalene is extracted through hydrogen peroxide oxidation, organic acid and inorganic acid catalysis, and distillation method.

  以上方法中,结晶法和分步结晶法因其高纯度和节能效果而被广泛应用。选择具体提取方法时,需要考虑原料来源、成本、环境影响及生产规模等因素。

  Among the above methods, crystallization and stepwise crystallization are widely used due to their high purity and energy-saving effects. When selecting a specific extraction method, factors such as raw material sources, costs, environmental impact, and production scale need to be considered.

  本文由精萘厂家为您提供,我们的网站是:http://www.jnjdbc.cn我们将以全心全意的热情为您提供服务,欢迎您的访问!

  This article is provided by the refined naphthalene manufacturer. Our website is: http://www.jnjdbc.cn We will provide you with wholehearted enthusiasm and welcome your visit!

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