济南聚大邦成化工有限公司
联系人:张总
电话:13583111587
网址:www.jnjdbc.cn
地址:济南市天桥区新材料市场南区7-1-1
精萘厂家:提取的方法
精萘的提取可以通过多种方法进行,以下是几种常见的精萘提取方法:
The extraction of refined naphthalene can be carried out through various methods, and the following are several common methods for extracting refined naphthalene:
煤焦油提取法 :
Coal tar extraction method:
从高温煤焦油中分离出萘油馏分(210-230℃),经过洗涤脱酚和精馏分离轻组分,得到工业萘。
Separate naphthalene oil fraction (210-230 ℃) from high-temperature coal tar, wash and dephenolate, and separate light components by distillation to obtain industrial naphthalene.
工业萘进一步通过酸洗和蒸馏,硫含量可降至小于0.1%,再通过加氢精制工艺,硫含量可低于0.05%。
Industrial naphthalene can further reduce its sulfur content to less than 0.1% through acid washing and distillation, and then through hydrogenation refining process, its sulfur content can be reduced to less than 0.05%.
结晶法 :
Crystallization method:
利用不同纯度萘的熔点差异,通过分步结晶和融化操作,高结晶点萘进入成品槽,低纯度萘进入残油罐。
By utilizing the melting point differences of different purity naphthalenes, high crystallization point naphthalenes enter the finished product tank and low purity naphthalenes enter the residual oil tank through step-by-step crystallization and melting operations.
在精制工序中,通过闪蒸进一步精制制得精萘。
In the refining process, refined naphthalene is further refined by flash evaporation.
溶剂萃取法 :
Solvent extraction method:
使用乙醇对煤焦油进行萃取,然后对萃出液减压蒸馏,得到含萘量较高的固液混合物,经过滤抽干得到粗萘。
Ethanol is used to extract coal tar, and then the extracted liquid is subjected to vacuum distillation to obtain a solid-liquid mixture with high naphthalene content. After filtration and dehydration, crude naphthalene is obtained.
水蒸汽蒸馏法 :
Steam distillation method:
建立水蒸汽蒸馏提纯粗萘的方法,所得精萘纯度可达99.48%,回收率在93%以上。
Establishing a method for steam distillation purification of crude naphthalene, the purity of refined naphthalene obtained can reach 99.48%, with a recovery rate of over 93%.
分步结晶法 :
Stepwise crystallization method:
将工业萘装入箱式结晶器中,根据萘中各馏分结晶点的差别进行分步结晶提纯。
Load industrial naphthalene into a box type crystallizer and perform step-by-step crystallization purification based on the differences in crystallization points of each fraction in naphthalene.
竖管式结晶法 :
Vertical tube crystallization method:
利用竖管式结晶器进行多级结晶过程,包括结晶、发汗和熔融步骤,生产出高纯度的精萘。
Using a vertical tube crystallizer for multi-stage crystallization process, including crystallization, sweating, and melting steps, high-purity refined naphthalene is produced.
反应与精馏结合法 :
Reaction and distillation combined method:
以工业萘为原料,通过过氧化氢氧化和有机酸、无机酸催化,结合精馏方法提取精萘。
Using industrial naphthalene as raw material, refined naphthalene is extracted through hydrogen peroxide oxidation, organic acid and inorganic acid catalysis, and distillation method.
以上方法中,结晶法和分步结晶法因其高纯度和节能效果而被广泛应用。选择具体提取方法时,需要考虑原料来源、成本、环境影响及生产规模等因素。
Among the above methods, crystallization and stepwise crystallization are widely used due to their high purity and energy-saving effects. When selecting a specific extraction method, factors such as raw material sources, costs, environmental impact, and production scale need to be considered.
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This article is provided by the refined naphthalene manufacturer. Our website is: http://www.jnjdbc.cn We will provide you with wholehearted enthusiasm and welcome your visit!
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精萘的提取可以通过多种方法进行,以下是几种常见的精萘提取方法: The extraction of refined naphthalene can be carried o...